Agilent Technologies 1100 Series Manual de Instruções

s1Agilent 1100 Series Capillary LC SystemSystem Manual

x 1100 Series Capillary LC System ManualcontentsASafety InformationGeneral 176Operation 176Safety Symbols 177Lithium Batteries Information 178Danish I

90 1100 Series Capillary LC System Manual5 Parts and MaterialsTabl e 32 Sampling unit for the micro autosamplerItem Description Part NumberMicro sampl

1100 Series Capillary LC System Manual 91Parts and Materials 5Micro Analytical Head AssemblyTabl e 33 Micro analytical head assemblyItem Description P

92 1100 Series Capillary LC System Manual5 Parts and MaterialsMicro Injection Valve AssemblyTabl e 34 Micro injection valve assemblyItem Description P

1100 Series Capillary LC System Manual 93Parts and Materials 5Thermostatted Micro Autosampler Cover PartsTabl e 35 Thermostatted micro autosampler cov

94 1100 Series Capillary LC System Manual5 Parts and MaterialsVial TraysTabl e 36 Thermostatted autosampler vial trays and tray baseItem Description P

1100 Series Capillary LC System Manual 95Parts and Materials 5Thermostatted Column CompartmentTable 37 gives an overview over the main assemblies of t

96 1100 Series Capillary LC System Manual5 Parts and MaterialsFigure 24 Thermostatted column compartment main assemblies1231456789

1100 Series Capillary LC System Manual 97Parts and Materials 5Micro Column Switching ValveTabl e 38 Micro column switching valveItem Description Part

98 1100 Series Capillary LC System Manual5 Parts and MaterialsThermostatted Column Compartment Sheet Metal KitTabl e 39 Thermostatted column compartme

1100 Series Capillary LC System Manual 99Parts and Materials 5Thermostatted Column Compartment Cover PartsTabl e 40 Thermostatted column compartment c

1Agilent 1100 Series Capillary LC SystemSystem ManualAgilent Technologies1Installing your Capillary LC SystemSite Requirements 2Physical Specification

100 1100 Series Capillary LC System Manual5 Parts and MaterialsThermostatted Column Compartment Leak PartsTabl e 41 Thermostatted column compartment l

1100 Series Capillary LC System Manual 101Parts and Materials 5Diode Array DetectorTable 42 gives an overview over the main assemblies of the diode ar

102 1100 Series Capillary LC System Manual5 Parts and MaterialsFigure 29 Diode array detector main assemblies641723985

1100 Series Capillary LC System Manual 103Parts and Materials 5DAD - Optical Unit AssemblyTable 43 gives an overview over optical unit parts:. The ite

104 1100 Series Capillary LC System Manual5 Parts and MaterialsFigure 30 Optical Unit Parts143572137141561089111216

1100 Series Capillary LC System Manual 105Parts and Materials 5500 nl Flow CellFigure 31 500 nl Flow CellTabl e 44 500 nl Flow Cell - partsItem Descri

106 1100 Series Capillary LC System Manual5 Parts and Materials12 Cell Seal Assembly 10 mm see kit below13 Quartz Cell Body 10 mm G1315-8000114 Handle

1100 Series Capillary LC System Manual 107Parts and Materials 5Fan Assembly PartsTabl e 45 Fan assembly partsItem Description Part Number1 Heater asse

108 1100 Series Capillary LC System Manual5 Parts and MaterialsHolmium Oxide FilterTabl e 46 Holmium oxide filter assembly partsItem Description Part

1100 Series Capillary LC System Manual 109Parts and Materials 5Diode Array Detector Cover PartsTabl e 47 Diode array detector cover partsItem Descript

2 1100 Series Capillary LC System Manual1 Installing your Capillary LC SystemSite RequirementsA suitable environment is important to ensure optimum pe

110 1100 Series Capillary LC System Manual5 Parts and MaterialsCommon PartsThis chapter shows the parts identification of the common parts like rear p

1100 Series Capillary LC System Manual 111Parts and Materials 5Rear panelTabl e 49 Rear panelItem Description Part Number1 Standoff — remote connector

112 1100 Series Capillary LC System Manual5 Parts and MaterialsPower and Status Light PipesTabl e 50 Power and status light pipesItem Description Part

1100 Series Capillary LC System Manual 113Parts and Materials 5Leak PartsTabl e 51 Leak partsItem Description Part Number1 Holder, leak funnel 5041-83

114 1100 Series Capillary LC System Manual5 Parts and MaterialsFoam partsSheet metal kitTabl e 52 Foam partsDescription Part numberFoam kit for the ca

1100 Series Capillary LC System Manual 115Parts and Materials 5Micro Degasser Accessory KitCapillary Pump Preventive Maintenance Kit G1376-68710Tabl e

116 1100 Series Capillary LC System Manual5 Parts and MaterialsCapillary Pump Accessory KitTabl e 56 Capillary pump accessory kit G1376-68705Descripti

1100 Series Capillary LC System Manual 117Parts and Materials 5Micro Well-plate Sampler Accessory Kit G1377-68705Tabl e 57 Micro well-plate sampler ac

118 1100 Series Capillary LC System Manual5 Parts and MaterialsThermostatted Micro Autosampler Accessory KitTabl e 58 Thermostatted micro autosampler

1100 Series Capillary LC System Manual 119Parts and Materials 5Column Compartment with Micro Column Selection Valve Accessory KitTabl e 59 Column comp

1100 Series Capillary LC System Manual 3Installing your Capillary LC System 1Bench SpaceThe modules dimensions and weight (see Table 2 on page 5) allo

120 1100 Series Capillary LC System Manual5 Parts and MaterialsDAD Accessory KitTabl e 60 DAD accessory kit G1315-68705Description Part NumberAccessor

1100 Series Capillary LC System Manual 121Parts and Materials 5CablesTable 61 offers an overview over all cables supplied:WARNINGNever use cables othe

122 1100 Series Capillary LC System Manual5 Parts and MaterialsBCD cables 3392/3 integrators 18594-605103396 integrator 03396-60560General purpose (sp

1100 Series Capillary LC System Manual 123Parts and Materials 5Analog CablesOne end of these cables provides a BNC connector to be connected to Agilen

124 1100 Series Capillary LC System Manual5 Parts and MaterialsRemote CablesOne end of these cables provides a Agilent Technologies APG (Analytical Pr

1100 Series Capillary LC System Manual 125Parts and Materials 5Tabl e 66 Agilent 1100 to 3390 integratorsConnector01046-60203Pin3390PinAgilent 1100Sig

126 1100 Series Capillary LC System Manual5 Parts and MaterialsTabl e 68 Agilent 1100 to 3394 integratorsConnector01046-60210Pin3394PinAgilent 1100Sig

1100 Series Capillary LC System Manual 127Parts and Materials 5Agilent 1100 to 3396 Series II / 3395A IntegratorsUse the cable 03394-60600 and cut pin

128 1100 Series Capillary LC System Manual5 Parts and MaterialsTabl e 70 Agilent 1100 to 3396 Series III / 3395B integratorsConnector03396-61010Pin33X

1100 Series Capillary LC System Manual 129Parts and Materials 5Tabl e 72 Agilent 1100 to HP 1090 LC, HP 1040 DAD or signal distribution moduleConnecto

4 1100 Series Capillary LC System Manual1 Installing your Capillary LC SystemPhysical SpecificationsTabl e 1 Common Physical SpecificationsType Specif

130 1100 Series Capillary LC System Manual5 Parts and MaterialsBCD CablesOne end of these cables provides a 15-pin BCD connector to be connected to th

1100 Series Capillary LC System Manual 131Parts and Materials 5Tabl e 75 Agilent 1100 to 3396 integratorsConnector03396-60560Pin3392/3PinAgilent 1100S

132 1100 Series Capillary LC System Manual5 Parts and MaterialsAuxiliary CableOne end of this cable provides a modular plug to be connected to the Agi

1100 Series Capillary LC System Manual 133Parts and Materials 5External Contact CableOne end of this cable provides a 15-pin plug to be connected to A

134 1100 Series Capillary LC System Manual5 Parts and MaterialsRS-232 Cable KitThis kit contains a 9-pin female to 9-pin female Null Modem (printer) c

135Agilent 1100 Series Capillary LC SystemSystem ManualAgilent Technologies6OptionsExtended Flow Range Kit (G1376-69707) 1360.1 - 2.5 ml/min Flow Capi

136 1100 Series Capillary LC System Manual6OptionsExtended Flow Range Kit (G1376-69707) The extended flow range kit described in Table 80 lets you ada

1100 Series Capillary LC System Manual 137Options 6Figure 39 Capillary pump flow diagramPump head BColumnInjection valveMixerSSVEMPVFlow sensorNeedleA

138 1100 Series Capillary LC System Manual6OptionsInstalling the Extended Flow Range Kit1 Using the 4 mm / 1/4 - 5/16 inch open wrenches disconnect th

1100 Series Capillary LC System Manual 139Options 60.1 - 2.5 ml/min Flow Capillary Kit (5065-4495)It is possible to use the capillary pump with a flow

1100 Series Capillary LC System Manual 5Installing your Capillary LC System 11100Tabl e 2 Module Specific SpecificationsAgilent 1100 Module Part Numbe

140 1100 Series Capillary LC System Manual6OptionsInstalling the 0.1 - 2.5 ml/min flow capillary kit1 Switch off the pump module.2 Disconnect the capi

1100 Series Capillary LC System Manual 141Options 612 Replace the loop capillary with the capillary G1329-87302 if you have a micro autosampler (G1389

142 1100 Series Capillary LC System Manual6Options..Tabl e 82 Pressure drop at 2.5 ml/min for different concentrations (no column)% of organic phase P

1100 Series Capillary LC System Manual 143Options 6Micro Column Switching Valve G1388A#055The micro column switching valve allows to work with 2 colum

144 1100 Series Capillary LC System Manual6OptionsThe micro column switching valve allows also to work with a column back-flushing. The sample is inje

1100 Series Capillary LC System Manual 145Options 6Parts Identification for Micro Column Switching ValveTabl e 84 Micro column switching valveItem Des

146 1100 Series Capillary LC System Manual6OptionsReplacing Rotor Seal of Micro Column Switching Valve15 Remove the stator head and the rotor seal.16

1100 Series Capillary LC System Manual 147Options 6Removing the Micro Column Switching ValveWhen required If valve failed or bottom foam part has to b

148 1100 Series Capillary LC System Manual6Options4 Lift the Z-panel together with the top plastic panel half-way out of the guide.5 Locate the ambien

1100 Series Capillary LC System Manual 149Options 68 Remove the Valve from its location. For the installation refer to “Installing the Micro Column Sw

6 1100 Series Capillary LC System Manual1 Installing your Capillary LC SystemSystem Installation ProcessDamaged PackagingIf the delivery packaging sho

150 1100 Series Capillary LC System Manual6OptionsInstalling the Micro Column Switching ValveWhen required For first time installation or after it was

1100 Series Capillary LC System Manual 151Options 63 Carefully insert the top plastic panel together with the Z-panel into the guide and press it half

152 1100 Series Capillary LC System Manual6Options7 Fix the Z-panel with the two screws. 8 Reconnect the grounding connection of the valve at the Z-pa

1100 Series Capillary LC System Manual 153Options 6500 nl Flow Cell Kit G1315-68714This section describes the 500 nl flow cell for Agilent 1100 Series

154 1100 Series Capillary LC System Manual6OptionsSpecial Information for MaintenanceThe supplied parts with the flow cell allow different fittings an

1100 Series Capillary LC System Manual 155Options 6The cell fittings are factory installed and tested for leakage. These connections should not be use

156 1100 Series Capillary LC System Manual6OptionsInstallation of the Flow CellThe flow cell is supplied with blank capillaries at the instrument side

1100 Series Capillary LC System Manual 157Options 6Step 3 and 4 have to be done for each of the two flow cell capillaries, if this connection type is

158 1100 Series Capillary LC System Manual6Options6 The figure below shows the sealing principle within the union “top seal”, hand tightened before to

1100 Series Capillary LC System Manual 159Options 69 Insert the PEEK capillaries from the flow cell body together with the SST fitting, ferrule and co

1100 Series Capillary LC System Manual 7Installing your Capillary LC System 1Installing a Capillary LC System with a Non-Thermostatted SamplerThese in

160 1100 Series Capillary LC System Manual6OptionsConnecting Small I.D. CapillariesColumns from e.g. LC Packings have capillary connections which are

1100 Series Capillary LC System Manual 161Options 6Replacing or Cleaning PartsCAUTIONThe quartz block can be cleaned with alcohol. DO NOT touch the in

162 1100 Series Capillary LC System Manual6Options5 The quartz body and the cell seal assembly can be separated for cleaning purpose.6 This figure sho

1100 Series Capillary LC System Manual 163Options 69 Insert the flow cell capillaries and tighten them fingertight.Use of the wrench and torque adapte

164 1100 Series Capillary LC System Manual6Options

165Agilent 1100 Series Capillary LC SystemSystem ManualAgilent Technologies7Performance SpecificationsPerformance Specifications Agilent 1100 Series C

166 1100 Series Capillary LC System Manual7 Performance SpecificationsPerformance Specifications Agilent 1100 Series Capillary PumpTabl e 86 Performan

1100 Series Capillary LC System Manual 167Performance Specifications 7Delay volume Typically 3 µl from the electronic flow control to the pump outlet

168 1100 Series Capillary LC System Manual7 Performance SpecificationsPerformance Specifications Agilent 1100 Series Micro Vacuum DegasserTabl e 88 Pe

1100 Series Capillary LC System Manual 169Performance Specifications 7Performance Specifications Agilent 1100 Series Thermostatted Micro AutosamplerTa

8 1100 Series Capillary LC System Manual1 Installing your Capillary LC SystemInstall the Diode Array Detector (DAD) (G1315B)Ensure the line power swit

170 1100 Series Capillary LC System Manual7 Performance SpecificationsPerformance specification Agilent 1100 Series Micro Well-plate SamplerTabl e 90

1100 Series Capillary LC System Manual 171Performance Specifications 7Performance Specifications Agilent 1100 Thermostatted Column Compartment.All spe

172 1100 Series Capillary LC System Manual7 Performance SpecificationsPerformance Specifications Agilent 1100 Series DADReference conditions for data

1100 Series Capillary LC System Manual 173Performance Specifications 7For specification on the 500 nl flow cell refer to Table 85 on page 153.Maximum

174 1100 Series Capillary LC System Manual7 Performance Specifications

175Agilent 1100 Series Capillary LC SystemSystem ManualAgilent TechnologiesASafety InformationThe following general safety precautions must be observe

176 1100 Series Capillary LC System ManualA Safety InformationGeneralThis is a Safety Class I instrument (provided with terminal for protective earthi

1100 Series Capillary LC System Manual 177Safety Information ACapacitors inside the instrument may still be charged, even though the instrument has be

178 1100 Series Capillary LC System ManualA Safety InformationLithium Batteries InformationDanish Information:.WARNINGDanger of explosion if battery i

1100 Series Capillary LC System Manual 179Safety Information ARadio InterferenceNever use cables other than the ones supplied by Agilent Technologies

1100 Series Capillary LC System Manual 9Installing your Capillary LC System 1Install the Thermostatted Column Compartment (TCC) (G1316A)1 Ensure the l

180 1100 Series Capillary LC System ManualA Safety Information• High concentrations of inorganic acids like nitric acid, sulfuric acid especially at h

1100 Series Capillary LC System Manual 181IndexNumerics500 nl flow cell, 153Aaccuracy of temperaturecolumn compartment, 171accuracy of wavelength, 172

182 1100 Series Capillary LC System ManualIndexMmaximum flow rate, 168metering seal, 81, 91micro column switching valve (optional)description, 143inst

1100 Series Capillary LC System Manual 183Indexsystem pressurehigh, 57low, 56unstable, 59system troubleshooting, 55TTCCinstalling, 9temperaturerange,

184 1100 Series Capillary LC System ManualIndex

' %%(&'' %%(&'G1388-90001s1In This BookThis manual contains technical reference information about the Agilent

ii 1100 Series Capillary LC System ManualNotices© Agilent Technologies, Inc. 2002No part of this manual may be reproduced in any form or by any means

10 1100 Series Capillary LC System Manual1 Installing your Capillary LC SystemInstall the Micro Well-plate Sampler (G1377A)1 Ensure the line power swi

1100 Series Capillary LC System Manual 11Installing your Capillary LC System 1Install the Capillary Pump (G1376A)1 Ensure the line power switch at the

12 1100 Series Capillary LC System Manual1 Installing your Capillary LC SystemInstall the Micro Vacuum Degasser (G1379A)1 Ensure the line power switch

1100 Series Capillary LC System Manual 13Installing your Capillary LC System 1Install the Solvent Cabinet1 Place the solvent cabinet on top of the deg

14 1100 Series Capillary LC System Manual1 Installing your Capillary LC SystemInstalling a Capillary LC System with a Thermostatted Micro SamplerThese

1100 Series Capillary LC System Manual 15Installing your Capillary LC System 1Install the Thermostat for 1100 Samplers (G1330B)1 Place the thermostat

16 1100 Series Capillary LC System Manual1 Installing your Capillary LC SystemInstall the Micro Sampler (G1387A Micro Autosampler (ALS), or G1378A Mic

1100 Series Capillary LC System Manual 17Installing your Capillary LC System 1Install the Thermostatted Column Compartment (TCC) (G1316A)1 Ensure that

18 1100 Series Capillary LC System Manual1 Installing your Capillary LC SystemInstall the Diode Array Detector (DAD) (G1315B)1 Ensure the line power s

1100 Series Capillary LC System Manual 19Installing your Capillary LC System 1Install the Capillary Pump (G1376A)1 Ensure the line power switch at the

1100 Series Capillary LC System Manual iiiIn This Manual…This manu

20 1100 Series Capillary LC System Manual1 Installing your Capillary LC SystemInstall the Micro Vacuum Degasser (G1379A)1 Ensure the line power switch

1100 Series Capillary LC System Manual 21Installing your Capillary LC System 1Install the Solvent Cabinet1 Place the solvent cabinet on top of the deg

22 1100 Series Capillary LC System Manual1 Installing your Capillary LC SystemGet the System Ready for the First InjectionWhen you are using the syste

1100 Series Capillary LC System Manual 23Installing your Capillary LC System 1Manually Priming the Solvent Channels.1 The degasser accessory kit conta

24 1100 Series Capillary LC System Manual1 Installing your Capillary LC SystemPurging the Pump1 Make sure that the 1/8 inch plastic waste tube is tigh

1100 Series Capillary LC System Manual 25Installing your Capillary LC System 1Conditioning the System Under Method ConditionsIf you wish to condition

26 1100 Series Capillary LC System Manual1 Installing your Capillary LC SystemInject the Check-out SampleThe purpose of the instrument check is to dem

1100 Series Capillary LC System Manual 27Installing your Capillary LC System 1Procedure1 Make a single injection of the isocratic test standard under

28 1100 Series Capillary LC System Manual1 Installing your Capillary LC System

29Agilent 1100 Series Capillary LC SystemSystem ManualAgilent Technologies2Optimizing PerformanceHints for Successful Use of the Capillary Pump 30Solv

iv 1100 Series Capillary LC System Manual

30 1100 Series Capillary LC System Manual2 Optimizing PerformanceHints for Successful Use of the Capillary PumpPump issues• Flush the pump extensively

1100 Series Capillary LC System Manual 31Optimizing Performance 2• To achieve the best flow stability, especially in the micro mode, %Ripple must be w

32 1100 Series Capillary LC System Manual2 Optimizing PerformanceSampler issues• For fast gradient use valve to bypass function after the sample is tr

1100 Series Capillary LC System Manual 33Optimizing Performance 2Solvent InformationAlways filter solvents through 0.4 µm filters, small particles can

34 1100 Series Capillary LC System Manual2 Optimizing PerformancePrevent Blocking of Solvent Inlet FiltersContaminated solvents or algae growth in the

1100 Series Capillary LC System Manual 35Optimizing Performance 2Cleaning the Solvent Filters• Remove the blocked solvent filter from the bottle-head

36 1100 Series Capillary LC System Manual2 Optimizing PerformanceHints for the Micro Vacuum DegasserIf you are using the vacuum degasser for the first

1100 Series Capillary LC System Manual 37Optimizing Performance 2When to use Alternative SealsThe standard seals for the capillary pump can be used fo

38 1100 Series Capillary LC System Manual2 Optimizing PerformanceHow to Choose the Primary FlowPrimary Flow is a parameter which exists only when the

1100 Series Capillary LC System Manual 39Optimizing Performance 2Fast Gradients range (800-1300 µl/min)In this range, the pump gradient delay time is

1100 Series Capillary LC System Manual vContents1 Installing your Capillary LC SystemSite Requirements 2Physical Specifications 4System Installation P

40 1100 Series Capillary LC System Manual2 Optimizing PerformanceStatic Mixer and FilterThe capillary pump is equipped with a static mixer and an inli

1100 Series Capillary LC System Manual 41Optimizing Performance 2How to Optimize the Compressibility Compensation SettingThe compressibility compensat

42 1100 Series Capillary LC System Manual2 Optimizing Performance5 Starting with a compressibility setting of 10 × 10-6/bar increase the value in step

1100 Series Capillary LC System Manual 43Optimizing Performance 2The Fast Composition Change/Reconditioning FunctionPurposeThe capillary pump and the

44 1100 Series Capillary LC System Manual2 Optimizing Performance2 When the Fast System Flush time has elapsed, the micro well-plate sampler needle is

45Agilent 1100 Series Capillary LC SystemSystem ManualAgilent Technologies3Capillaries and FittingsCapillary Flow Diagram 46Connecting capillaries for

46 1100 Series Capillary LC System Manual3 Capillaries and FittingsCapillary Flow DiagramThe flow diagram in Figure 2 gives an overview of the capilla

1100 Series Capillary LC System Manual 47Capillaries and Fittings 3Connecting capillaries for the capillary LC system† SST: stainless steel* * PFS: Pe

48 1100 Series Capillary LC System Manual3 Capillaries and Fittings* PFS: Peek coated fused silica.*PFS: Peek coated fused silicaTabl e 8 Specific cap

1100 Series Capillary LC System Manual 49Capillaries and Fittings 3† SST: Stainless steel* * PFS: Peek coated fused silicaDescriptionsto Table 1 01 T

vi 1100 Series Capillary LC System Manualcontents2 Optimizing PerformanceHints for Successful Use of the Capillary Pump 30Pump issues 30Fused Silica C

50 1100 Series Capillary LC System Manual3 Capillaries and FittingsTabl e 11 Specific capillaries for use with a micro CSV and a 20 µl flow sensorFrom

1100 Series Capillary LC System Manual 51Capillaries and Fittings 3Figure 3 Micro column switching valve connections1234To det e c t o rFrom injection

52 1100 Series Capillary LC System Manual3 Capillaries and FittingsFittings and FerrulesTabl e 14 Fittings and ferrulesFitting Typ eName Description

1100 Series Capillary LC System Manual 53Capillaries and Fittings 3Instructions to connect a capillary.With Swagelock fitting (type A)• Slide the nut,

54 1100 Series Capillary LC System Manual3 Capillaries and FittingsHints for Successful use of Capillaries and Fittings• Never overtighten a fitting.•

55Agilent 1100 Series Capillary LC SystemSystem ManualAgilent Technologies4Basic System TroubleshootingSystem Pressure Abnormally Low 56System Pressur

56 1100 Series Capillary LC System Manual4 Basic System TroubleshootingSystem Pressure Abnormally LowSymptoms: The current system pressure is signific

1100 Series Capillary LC System Manual 57Basic System Troubleshooting 4System Pressure Abnormally HighSymptoms: The current system pressure is signifi

58 1100 Series Capillary LC System Manual4 Basic System TroubleshootingEMPV failed to initialize (micro mode only)Symptoms: An attempt to pump in the

1100 Series Capillary LC System Manual 59Basic System Troubleshooting 4Unstable column flow and/or system pressureSymptoms: In the micro mode, the pum

contents1100 Series Capillary LC System Manual vii4 Basic System TroubleshootingSystem Pressure Abnormally Low 56System Pressure Abnormally High 57EMP

60 1100 Series Capillary LC System Manual4 Basic System TroubleshootingDirty solvent inlet filters. Solvent intake is being restricted. %Ripple might

1100 Series Capillary LC System Manual 61Basic System Troubleshooting 4Poor peak shapeSymptoms: The peak shape has taken on a fronting or tailing char

62 1100 Series Capillary LC System Manual4 Basic System TroubleshootingFailure to produce peaks, or abnormally small peaks, after injectionSymptoms: T

1100 Series Capillary LC System Manual 63Basic System Troubleshooting 4Wandering Detector BaselineCritical Decision Determine if the problem is in the

64 1100 Series Capillary LC System Manual4 Basic System TroubleshootingUser interface displays error messages for specific modulesUnstable flow and/or

65Agilent 1100 Series Capillary LC SystemSystem ManualAgilent Technologies5Parts and MaterialsMicro Vacuum Degasser 66,Capillary Pump 69,Micro Well-pl

66 1100 Series Capillary LC System Manual5 Parts and MaterialsMicro Vacuum Degasser Table 16 gives an overview over the main assemblies:Tabl e 16 Micr

1100 Series Capillary LC System Manual 67Parts and Materials 5Figure 4 Micro vacuum degasser main assemblies991112345678

68 1100 Series Capillary LC System Manual5 Parts and MaterialsMicro Vacuum Degasser Cover PartsFigure 5 Micro vacuum degasser cover partsTabl e 17 Mic

1100 Series Capillary LC System Manual 69Parts and Materials 5Capillary Pump Table 18 gives an overview over the main assemblies of the capillary pump

viii 1100 Series Capillary LC System ManualcontentsVial Trays 94Thermostatted Column Compartment 95Micro Column Switching Valve 97Thermostatted Column

70 1100 Series Capillary LC System Manual5 Parts and MaterialsFigure 6 Capillary pump main assembly7912135264108111314

1100 Series Capillary LC System Manual 71Parts and Materials 5Solvent Cabinet and Bottle Head AssemblyFigure 7 Solvent cabinet and bottle head assembl

72 1100 Series Capillary LC System Manual5 Parts and MaterialsCapillary Pump Hydraulic PathTabl e 20 Capillary pump hydraulic pathItem Description Par

1100 Series Capillary LC System Manual 73Parts and Materials 5Figure 8 Capillary pump hydraulic path8109111234567

74 1100 Series Capillary LC System Manual5 Parts and MaterialsPump-Head AssemblyTabl e 21 Pump-head assemblyItem Description Part NumberPump head asse

1100 Series Capillary LC System Manual 75Parts and Materials 5Figure 9 Pump head assembly1235671194810

76 1100 Series Capillary LC System Manual5 Parts and MaterialsCapillary pump cover partsTable 22 gives an overview over the cover parts of the capilla

1100 Series Capillary LC System Manual 77Parts and Materials 5Micro Well-plate SamplerFigure 11 Micro well-plate sampler main assemblies67532913112810

78 1100 Series Capillary LC System Manual5 Parts and MaterialsTabl e 23 Micro well-plate sampler main assembliesItem Description Part Number1 Ribbon C

1100 Series Capillary LC System Manual 79Parts and Materials 5Sampling Unit for the Micro Well-plate SamplerFigure 12 Sampling unit for the micro well

contents1100 Series Capillary LC System Manual ixCAN Cable 132External Contact Cable 133RS-232 Cable Kit 134LAN Cables 1346OptionsExtended Flow Range

80 1100 Series Capillary LC System Manual5 Parts and MaterialsTabl e 24 Sampling unit for the micro well-plate samplerItem Description Part NumberSamp

1100 Series Capillary LC System Manual 81Parts and Materials 5Micro Analytical Head AssemblyTabl e 25 Micro analytical head assemblyItem Description P

82 1100 Series Capillary LC System Manual5 Parts and MaterialsMicro Injection Valve AssemblyNote : Tabl e 26 Micro injection valve assemblyItem Descri

1100 Series Capillary LC System Manual 83Parts and Materials 5Micro Well-plate Sampler - Vial TraysTabl e 27 Micro well-plate sampler vial trays and t

84 1100 Series Capillary LC System Manual5 Parts and MaterialsTabl e 28 Recommended plates and closing matDescription Rows Columns Plate height Volum

1100 Series Capillary LC System Manual 85Parts and Materials 5Micro Well-Plate Sampler Cover PartsTabl e 29 Micro well-plate sampler cover partsItem D

86 1100 Series Capillary LC System Manual5 Parts and MaterialsThermostatted Micro AutosamplerTable 30 offers an overview over the main assemblies of t

1100 Series Capillary LC System Manual 87Parts and Materials 5Figure 17 Thermostatted micro autosampler main assemblies765321948101112

88 1100 Series Capillary LC System Manual5 Parts and MaterialsThermostat for 1100 Samplers Figure 18 ThermostatTabl e 31 Thermostat for micro autosamp

1100 Series Capillary LC System Manual 89Parts and Materials 5Sampling Unit for the Micro AutosamplerFigure 19 offers an overview over the main assemb