Agilent Technologies 1100 Series Manual do Utilizador

saAgilent 1100 SeriesHPLC Value SystemUser’s Guide

10General information about your systemSystem ConfigurationSystem ConfigurationManual - isocratic HPLC System G1380AAstandard configuration • G1310A i

11General information about your systemSystem RestrictionsSystem RestrictionsThe system mentioned on page 10 has some restrictions compared to the sta

12General information about your systemSite RequirementsSite RequirementsA suitable environment is important to ensure optimum performance of the syst

13General information about your systemSite RequirementsBench SpaceThe modules’ dimensions and weight (see Table 2 on page 14) allow to place the modu

14General information about your systemPhysical SpecificationsPhysical SpecificationsFor your PC specifications refer to its documentation.Table 2 Phy

15General information about your systemPerformance SpecificationsPerformance SpecificationsThe performance specifications can be derived from the modu

16General information about your systemUser DocumentationUser DocumentationThe user documentation (aside from this System Manual) is provided as Acrob

22 Installing your SystemHow to install your system

18Installing your SystemUnpacking the ModulesUnpacking the ModulesDamaged PackagingIf the delivery packaging shows signs of external damage, please ca

19Installing your SystemInstalling the JetDirect card into the VW detectorInstalling the JetDirect card into the VW detectorThe 1100 series VW detecto

Agilent TechnologiesHewlett-Packard-Strasse 876337 WaldbronnGermany Copyright Agilent Technologies 1999All rights reserved. Reproduction, adaption, o

20Installing your SystemChoose the optimal stack configurationChoose the optimal stack configurationFigure 2 You can ensure optimum performance by ins

21Installing your SystemInstalling the Manual Injector and 1100 series HPLC modulesInstalling the Manual Injector and 1100 series HPLC modulesNOTE Ass

22Installing your SystemInstalling the Manual Injector and 1100 series HPLC modulesFigure 4 Installing the Manual Injector5 Install other system modul

23Installing your SystemInstalling the Manual Injector and 1100 series HPLC modules6 Connect the position-sensor cable to the start cable (see Figure

24Installing your SystemFlow Connections at the Manual InjectorFlow Connections at the Manual InjectorWARNING When opening capillary or tube fittings,

25Installing your SystemFlow Connections at the Manual InjectorFigure 8 Vent CapillariesLeak Drainage of the Manual InjectorWARNING Check the manual i

26Installing your SystemFlow Connections at the Isocratic PumpFlow Connections at the Isocratic PumpWARNING When opening capillary or tube fittings, s

27Installing your SystemFlow Connections at the Isocratic PumpFigure 10 Flow Connections of the Isocratic PumpBottle-head assemblySolvent tubeOutlet c

28Installing your SystemFlow Connections to the VW DetectorFlow Connections to the VW DetectorWARNING When opening capillary or tube fittings, solvent

29Installing your SystemFlow Connections to the VW DetectorFigure 11 Flow connections to the VW detectorNOTE If you add a Thermostatted Column Compart

User’s GuideAgilent 1100 Series HPLC Value System

30Installing your SystemInstalling the ChemStation HardwareInstalling the ChemStation Hardware1 Place the Value Solution ChemStation PC next to 1100 s

31Installing your SystemBooting the PC for the First TimeBooting the PC for the First TimeThe Value Solution ChemStation PC has been factory pre-confi

32Installing your SystemInstalling the LAN CommunicationInstalling the LAN CommunicationYour instrument HPLC system is operated via a standard LAN cro

33Installing your SystemInstalling the LAN CommunicationFigure 13 Bootp Server 4 Select Configure -> Add Entry to configure the Bootp Manager. The

34Installing your SystemInstalling the LAN CommunicationFigure 15 Bootp Manager8 Press Apply to activate the changes. The Bootp Manager now shows the

35Installing your SystemConfiguring the Analytical SystemConfiguring the Analytical SystemThis chapter describes how to configure the communication of

36Installing your SystemConfiguring the Analytical System2 Start the ChemStation Configuration Editor (see Figure 17) and type in the IP address of th

37Installing your SystemConfiguring the Analytical System5 When you start the Instrument 1 Online Value Solution ChemStation for the first time (refer

38Installing your SystemConfiguring the Analytical SystemFigure 21 shows the initial Value Solution ChemStation screen.Figure 21 ChemStation Online En

33 Setting up an AnalysisHow to analyze the isocratic standard sample using a single injection analysis

4 In This BookThis manual contains technical information about the Agilent 1100 Series HPLC Value System. The manual describes the following:• system

40Setting up an AnalysisThis chapter can be used for three purposes: • preparing the system, • to learn the set up of an HPLC analysis and • to use i

41Setting up an AnalysisBefore Using the SystemBefore Using the SystemSolvent InformationObserve recommendations on the use of solvents in chapter “So

42Setting up an AnalysisBefore Using the SystemNOTE The pump should never be used for priming empty tubings (never let the pump run dry). Use a syring

43Setting up an AnalysisRequirements and ConditionsRequirements and ConditionsWhat You Will NeedTable 6 lists the items you need to have for the set u

44Setting up an AnalysisRequirements and ConditionsTypical ChromatogramA typical chromatogram for this analysis is shown in Figure 22 on page 44. The

45Setting up an AnalysisPreparing the HPLC SystemPreparing the HPLC System1 Turn on the Value Solution ChemStation PC and the monitor.2 Start the Boot

46Setting up an AnalysisPreparing the HPLC System6 Purge the pump. For more information see “Priming and Purging the System” on page 41.7 Allow the de

47Setting up an AnalysisPreparing the HPLC System10 Click on the pump and VW detector icon (Figure 24 on page 46) to open the Setup of those modules.

48Setting up an AnalysisPreparing the HPLC System12 Click the button and select Change... to open the Signal Plot information. Select the Isocratic

49Setting up an AnalysisPreparing the HPLC System13 If both baselines are stable, set the Y-range for the VWD signal to 300 mAU. 14 Select the menu it

Contents51 General information about your systemSystem Configuration 1010System Restrictions 11Site Requirements 12Physical Specifications 14Performan

50Setting up an AnalysisRunning the Sample and Verifying the ResultsRunning the Sample and Verifying the Results1 At the Manual Injector move the hand

44 Troubleshooting your SystemIntroduction to the diagnostic features built into your system

52Troubleshooting your SystemThis chapter will introduce you to the diagnostic features built into your system. It is an overview and more details can

53Troubleshooting your SystemDiagnostic FunctionsDiagnostic FunctionsStatus Information on the 1100 ModulesLEDsThe 1100 modules provide two LEDs each.

54Troubleshooting your SystemOnline System InformationOnline System InformationOnline MessagesThe user interface (Value Solution ChemStation or Contro

55Troubleshooting your SystemOnline System InformationFigure 30 Online System Information Not Ready Information Instrument ActualsInstrument Logbook

56Troubleshooting your SystemInstrument Logbook and Help InformationInstrument Logbook and Help InformationThe user interface (Value Solution ChemStat

57Troubleshooting your SystemUsing Module DiagnosisUsing Module DiagnosisSelect View Diagnosis. Figure 32 shows the VW detector detailed diagnostic sc

58Troubleshooting your SystemUsing Module TestsUsing Module TestsSelect Show Module Tests. Figure 33 shows the VW detector module test screen. From th

59Troubleshooting your SystemProblems during the InstallationProblems during the InstallationIn case of problems during the installation follow the hi

6Contents3 Setting up an AnalysisBefore Using the System 41Solvent Information 41Priming and Purging the System 41Requirements and Conditions 43What Y

60Troubleshooting your SystemProblems during the Installation

55 Repair and MaintenanceWhat you should know about your system

62Repair and MaintenanceRepair and Parts Information for the 1100 series HPLC ModulesRepair and Parts Information for the 1100 series HPLC ModulesTher

63Repair and MaintenanceFirmware Update on 1100 ModulesFirmware Update on 1100 ModulesThe installation of new firmware is required • if a new version

64Repair and MaintenanceDeinstallation and Reinstallation of the ChemStationDeinstallation and Reinstallation of the ChemStationThe reinstallation of

65Repair and MaintenanceRecovering from an Operating System CrashRecovering from an Operating System CrashThe re-installation of the complete operatin

66Repair and MaintenanceRecovering from an Operating System Crash4 The PC will reboot and stop at the Login Information screen. The pre-configured use

67Repair and MaintenanceRecovering from an Operating System CrashFigure 36 TCP/IP Configuration Screens- Adapters Figure 37 TCP/IP Configuration Scree

68Repair and MaintenanceRecovering from an Operating System Crash5 Select No to the usage of DHCP and use C:\I386 as the location of your Windows NT 4

69Repair and MaintenanceRecovering from an Operating System CrashStep 3: Re-installation of Windows NT Service PackNOTE After the PC has been re-start

Contents7Step 1: Installation of Windows NT 65Step 2: Installation of TCP/IP protocol 66Step 3: Re-installation of Windows NT Service Pack 69Step 4: I

70Repair and MaintenanceRecovering from an Operating System Crash1 Open the Bootp Server window by clicking on it in the task bar.2 Now turn on the VW

71Repair and MaintenanceRecovering from an Operating System CrashFigure 40 Add Bootp Entry5 Exit with OK.6 Select Configure -> Bootp Manager. All e

72Repair and MaintenanceRecovering from an Operating System CrashFigure 42 Bootp Server - 1100 module found

Index73Numerics1100 Seriescontroller area network (CAN), 35Aaddingthe licence number, 36analog signals, 53, 54APG-remote, 23Bbooting the PC, 31CCAN110

74 IndexWwarranty and legal, 15weight, 14

In This BookThis manual contains technical reference information about the Agilent 1100 Series HPLC value system. The manual describes the following:•

8Contents

11 General information about your systemWhat you should know about your system