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170 1100 Series Capillary LC System Manual

7 Performance Specifications

Performance specification Agilent 1100 Series Micro Well-plate Sampler

Tabl e 90 Performance specifications Agilent 1100 series micro well-plate sampler

Type Specification

GLP features Early maintenance feedback (EMF), electronic records of

maintenance and errors

Communications Controller-area network (CAN). RS232C, APG-remote standard,

optional four external contact closures and BCD vial number output

Safety features Leak detection and safe leak handling, low voltages in maintenance

areas, error detection and display

Injection range 0.01 – 8 µl in 0.01 µl increments with the small loop capillary

0.01 – 40 µl in 0.01 µl increments with the extended loop capillary

Precision Typically < 0.5 % RSD of peak areas from 5 – 40 µl,

Typically <1%RSD from 1–5µl

Typically <3%RSD from 0.2–1µl

Sample viscosity range 0.2 – 5 cp

Sample capacity 2 × well-plates (MTP) + 10 × 2 ml vials

100 x 2 ml in one tray

40 x 2 ml in half tray

Injection cycle time Typically < 30 s using following standard conditions:

Default draw speed: 4 µl/min

Default eject speed: 10 µl/min

Injection volume: 0.1 µl

Carry-over Typically < 0.05 % using the following conditions:

Column: 150 x 0.5 mm Hypersil ODS, 3 µm

Mobile phase: Water/Acetonitrile = 85/15

Column Flow rate: 13 µl/min

Injection volume: 1 µl caffeine (=25ng caffeine), 1 µl water to test

carryover

Outside wash of needle before injection: 20 sec with water using

flush port

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