Agilent Technologies 1100 Series Manual do Utilizador descarregar pdf (Página 43)

Setting up an Analysis

Requirements and Conditions

What You Will Need

Table 6 lists the items you need to have for the set up of the analysis. Some of

these are optional (not required for the basic system).

Conditions

A single injection of the isocratic test standard is made under the conditions

given in Table 7:

Table 6 What you will need

HP 1100 Instrument Isocratic pump

Manual Injector

Detector - VWD, Standard flow cell installed

ChemStation or Control Module (optional)

Column: Zorbax Eclipse XDB-C8 150 x 4.6 mm i.d.

Part No. 993967-902 or Part No. 5063-6600

Standard: Part No. 01080-68704

0.15 wt.% dimethylphthalate, 0.15 wt.% diethylphthalate,

0.01 wt.% biphenyl, 0.03 wt.% o-terphenyl in methanol

Table 7 Conditions

Flow: 1.5 ml/minute

Stoptime: 6 minutes

Solvent: 100% (30% water/70% Acetonitrile)

Temperature Ambient

Wavelength VWD: 254 nm

Injection Volume 2 µl (VWD)

1 2 ... 38 39 40 41 42 43 44 45 46 47 48 ... 75 76

Sem comentários

Agilent Technologies 1100 Series Manual do Utilizador Página 43