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16 8000 Operator’s Manual
2 Introduction
The 8000 Dissolution Sampling Station provides an unattended solution
for automated sampling from a dissolution apparatus. The instrument
may be configured to control any instrument setup with a USP apparatus
1 (Baskets), 2 (Paddles), 3 (Reciprocating Cylinder), 5 (Paddle over
Disk), 6 (Rotating Cylinder), or 7 (Reciprocating Holder) offered by
Agilent Technologies, Inc. The firmware can store up to 15 different
sampling programs. Dissolution apparatus parameters are entered as
part of the 8000 program. These parameters are downloaded to the
dissolution apparatus when beginning a test with the 8000.
The 8000 fail-safe sample delivery uses either the 810 Peristaltic Pump
or 806 Syringe Pump optionally coupled with the automated 808 Filter
Changer. Hard-copy documentation is provided by the built-in Report
Center Printer which prints all essential parameters for proof of proper
operation and compliance with current GMPs.
The 8000 may be configured with a replacement media (RM) module
which replenishes any sample volume removed with fresh media.
Sample is delivered into test tubes or pre-capped HPLC autosampler
vials for direct transfer of samples to an HPLC system. Sample trays are
available in a variety of sizes to accommodate various sizes of vials or
test tubes.
The 8000 is automation ready. An RS232 port permits integration with
other automated systems. Sampling runs can be activated with an
external switch closure or TTL signal. The 8000 has a programmable
TTL output to control the instruments in the system.
- Agilent 8000 1
- Dissolution Sampling 1
- Contents 3
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- 8000 Operator’s Manual 5 5
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- 8000 Operator’s Manual 7 7
- 8 8000 Operator’s Manual 8
- 8000 Operator’s Manual 9 9
- 10 8000 Operator’s Manual 10
- Electrical Hazards 12
- Information Symbols 14
- Introduction 15
- 8000 with Peristaltic Pump 17
- CC1234xxxx 18
- Setting Up the 8000 19
- Unpacking Your 8000 21
- Installation 22
- Setup of 8000 and Components 34
- Installing the Sample Tray 36
- (Peristaltic Pump only) 37
- Installing the RM Module 38
- External Unit 39
- Hidden Key Functions 41
- 42 8000 Operator’s Manual 42
- 3 Setting Up the 8000 42
- Table 1 Hidden Key Functions 42
- Setting Up the 8000 3 43
- 8000 Operator’s Manual 43 43
- 44 8000 Operator’s Manual 44
- Operating the 8000 45
- 8000 Keypad Options 46
- Operating the 8000 4 47
- 8000 Operator’s Manual 47 47
- Main Menu 48
- 8000 Operator’s Manual 49 49
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- 60 8000 Operator’s Manual 60
- Creating a Sample Program 61
- 8000 Operator’s Manual 63 63
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- SAMPLE TIME POINT: 000:02 65
- Starting a 8000 Program 66
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- DISSO Options Screen 69
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- ON R-M PUMP displays 84
- 8000 Operator’s Manual 85 85
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- 8000 Operator’s Manual 89 89
- Starting a Program 91
- APP 3/7 Options Screen 93
- 94 8000 Operator’s Manual 94
- Table 2 4 App 3/7 Options 94
- Manual Sample 95
- 96 8000 Operator’s Manual 96
- Automatic Calibration 97
- 1 MANUAL 2 AUTOMATIC 98
- Manual Calibration 99
- Daisy Chaining 102
- 104 8000 Operator’s Manual 104
- 4 Operating the 8000 104
- Agilent Technologies 105
- Preventive Maintenance 106
- Apparatus 3 / 7 107
- Start Immediately 108
- Programmed Clean 108
- Apparatus 1 / 2 111
- Syringe and Seal Replacement 112
- Cleaning the Syringes 113
- Filter Changer (optional) 115
- Report Center Impact Printer 119
- Replacing a Paper Roll 120
- Toggling Your Printer Online 121
- Printer Self Test 121
- Printer Configuration 122
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