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272
Reference Manual
Agilent 1100 Series
Quaternary Pump
1
2
3
4
5
6
7
8
...
271
272
Agilent 1100 Series
1
Quaternary Pump
1
Reference Manual
1
Contents
10
Radio Interference 264
11
Sound Emission 264
11
Solvent Information 265
11
1 Installing the Pump
13
Site Requirements
14
Bench Space
15
Environment
15
°C (41–131 °F)
16
°C (-4–158 °F)
16
°C (77–104 °F)
16
Unpacking the Quaternary Pump
17
ESD: Electrostatic Discharge
18
Power Switch
22
Serial number
22
Installing the Pump
27
2 Optimizing Performance
31
Optimizing Performance
33
Procedure” on page 112)
33
Degasser
36
Gradient Valve (MCGV)
37
When to Use Alternative Seals
39
Optimize the Compressibility
40
Compensation Setting
40
3 Troubleshooting and
43
Test Functions
43
Troubleshooting and Test
44
Functions
44
Status Indicators
45
Power Supply Indicator
46
Pump Status Indicator
46
Error Messages
47
Timeout
48
Shut-Down
49
Remote Timeout
50
Synchronization Lost
51
Leak Sensor Open
53
Leak Sensor Short
54
Compensation Sensor Open
55
Compensation Sensor Short
56
Fan Failed
57
Open Cover
58
Restart Without Cover
59
Zero Solvent Counter
60
Pressure Above Upper Limit
61
Pressure Below Lower Limit
62
Pressure Signal Missing
63
Missing Pressure Reading
64
Pump Configuration
65
Valve Fuse
66
Inlet-Valve Fuse
67
Valve Failed
68
Motor-Drive Power
69
Encoder Missing
70
Inlet-Valve Missing
71
Temperature Out of Range
72
Temperature Limit Exceeded
73
Servo Restart Failed
74
Pump Head Missing
75
Index Limit
76
Index Adjustment
77
Index Missing
78
Stroke Length
79
Initialization Failed
80
Wait Timeout
81
Pressure Test
82
Positioning the blank nut
83
Running the Pressure Test
84
Evaluating the Results
86
Leak Test
88
Running the Leak Test
90
All plateaus negative
94
Ramp 3 does not reach limit
95
4 Repairing the Pump
97
Cleaning the Quaternary Pump
99
Using the ESD Strap
100
Overview
101
Simple Repair Procedures
102
Valve cartridge
104
Valve body
104
Repairing the Pump
105
Gold seal
106
Plastic cap
106
Purge Valve
108
Purge valve
109
Pump outlet capillary
109
Waste tube
109
Head Assembly
110
Wear-in Procedure
112
Seal Wear-in Procedure
113
Exchanging the Plungers
115
Pump head screws
116
Pump head
116
Lock screw
116
Exchanging the Wash Seals
119
Insert tool
120
Support ring
120
Plunger housing
121
Balls of spindle drive
122
Metering drive
122
Pumphead screws
122
Valve (MCGV)
123
BCD (Interface) board
126
Exchanging Internal Parts
127
Clip fastener (1)
128
Light light switch
130
Top foam cover
130
Foam lever
130
Board (LPM Board)
131
Screws and Nut
132
Analog output
132
Board recessBoard recess
132
Entering the Type Command
134
Entering the Serial Number
135
Exchanging the Damper
138
Reconnect
140
Exchanging the Fan
141
Figure 22 Exchanging the Fan
142
Exchanging the Pump Drive
143
Exchanging the Power Supply
147
Power supply screws
148
Light pipe
149
Exchanging the Leak Sensor
152
Assembling the Main Cover
155
Light switch
156
Holding
157
Leak funnel
158
Waste tube holder
158
5 Parts and Materials
159
Overview of Main Assemblies
160
Parts and Materials
161
Control Module (B-version)
163
Solvent Cabinet
164
Bottle Head Assembly
165
Hydraulic Path
166
Cover Parts
167
Sheet Metal Kit
168
Foam Parts
169
Power and Status Light Pipes
170
Leak Parts
171
Pump Head Assembly
172
Figure 35 Pump Head Assembly
173
Outlet Ball Valve Assembly
176
Purge Valve Assembly
177
Active Inlet Valve Assembly
178
Accessory Kit G1311-68705
179
Reorder number (pack of 3)
180
Reorder number (pack of 10)
180
Cable Overview
181
Analog Cables
183
Agilent 1100 to BNC Connector
184
Remote Cables
185
BCD Cables
190
Auxiliary Cable
192
CAN Cable
192
External Contact Cable
193
RS-232 Cable Kit
194
LAN Cables
195
6 Introduction to the
197
Quaternary Pump
197
How does the Pump Work?
200
Electrical Connections
204
Instrument Layout
206
EMF Counters
207
Using the EMF Counters
208
The Electronics
209
Firmware Description
214
Firmware Updates
215
Optional Interface Boards
216
LAN Board
217
Analog Signal Output
219
GPIB Interface
219
CAN Interface
219
APG Remote Interface
220
Instrument
222
GPIB Default Addresses
224
Forced Cold-Start Settings
226
Stay Resident Settings
226
Mode Select12345678
227
TEST/BOOT11001000
227
7 Control Module Screens
231
Diagnostics and Tests
251
8 Specifications
253
Performance Specifications
254
Specifications
255
Warranty Statement
257
Safety Information
260
Safety Symbols
261
Lithium Batteries Information
263
Radio Interference
264
Sound Emission
264
Solvent Information
265
In This Book
272
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